顶空进样气相色谱质谱法同时检测食品包装材料中的10种残留溶剂

顶空进样气相色谱质谱法同时检测食品包装材料中的10种残留溶剂
目的  建立顶空气相色谱-质谱检测食品包装材料中10种残留有机溶剂的分析方法。方法  采用GC-MS选择离子监测(SIM)模式进行定量分析。结果  10种溶剂在0.001~0.1 mg/m2浓度范围线性关系良好, 相关系数在0.9999~1.0000, 对最低浓度点进行了重现性实验, RSD均小于10%, 回收率79.0%~106.2%, 精密度1.08％~8.02％。结论  此方法快速、准确可以满足国内外对食品包装材料中10种残留有机溶剂的同时检测。

Objective  To establish a method for the determination of 10 residual solvents released from the food packaging material by the headspace gas chromatography-mass spectrometry. Methods  The method was established by gas chromatography mass spectrum with selected ion monitor (GC-MS/SIM). Results  The linear range of 10 residual solvents were 0.001~0.1 mg/m2 with correlative coefficient of0.9999~1.00000. The coefficient of variation was<10% on the lowest concentration. The average recoveries were 79.0％~106.2％ with the relative standard deviations (RSD) of 1.08％~8.02％. Conclusion  This analysis method is rapid and accurate, and it can be used for the simultaneous determination of 10 residual solvents released from the food packaging material.

标题：顶空进样气相色谱质谱法同时检测食品包装材料中的10种残留溶剂
英文标题：Determination of 10 residual solvents in food packaging material by headspace gas chromatography-mass spectrometry

作者：
刘宝圣 河北出入境检验检疫局
段永生 河北出入境检验检疫局
马育松 河北出入境检验检疫局
郭春海 河北出入境检验检疫局

中文关键词:食品包装材料,溶剂残留,顶空气相色谱质谱(HS-GC/MS),选择离子扫描(SIM),
英文关键词:food packaging material,residual solvents,headspace-gas chromatography/mass spectrometry,selected ion monitoring,

发表日期：2013-09-17

顶空进样气相色谱质谱法同时检测食品包装材料中的10种残留溶剂.pdf

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