山茶油多元掺假近红外模型的建立与研究
山茶油多元掺假近红外模型的建立与研究
目的建立基于近红外光谱结合偏最小二乘法的山茶油、花生油和玉米油多元掺假模型。方法通过对比不同建模光谱波段、预处理方法对模型进行优化研究, 确定最优的山茶油、花生油和玉米油多元掺假模型。结果所建模型性能指数均大于0.99, 校正集和预测集的均方差在0.6以内。经未知掺假样品的外部验证, 预测值与实测值之间有较好的相关性, 二元掺假模型预测值的相对误差在1%以内, 三元掺假在6%以内, 验证结果良好。结论近红外光谱结合偏最小二乘法的检测技术快速、有效、环保, 可用于定量检测山茶油的掺假。
ObjectiveTo establish a multiple adulteration model of camellia oil, peanut oil and corn oil based on near-infrared spectroscopy combined with partial least squares method. MethodsThe model was optimized by comparing different spectral bands and pretreatment methods. The optimal multiple adulteration model of camellia oil, peanut oil and corn oil was determined. ResultsThe performance indexes of the models were all greater than 0.99, and the mean variance of the correction set and prediction set was within 0.6. After the external verification of unknown adulteration samples, there was a good correlation between the predicted value and the measured value. The relative error of the predicted value of the binary adulteration model was within 1%, the ternary adulteration was within 6%, and the verification results are good. ConclusionNear-infrared spectroscopy combined with partial least square method is fast, effective and environmentally friendly, which can be used for quantitative detection of adulteration of camellia oil.
标题：山茶油多元掺假近红外模型的建立与研究
英文标题：Establishment and study of camellia oil multiple adulterationnear-infrared model
作者：
姚婉清 嘉应学院化学与环境学院
彭梦侠 嘉应学院化学与环境学院
陈梓云 嘉应学院化学与环境学院
张家蔓 嘉应学院化学与环境学院
林量谦 嘉应学院化学与环境学院
甘海昌 嘉应学院化学与环境学院
中文关键词:山茶油,掺假检测,近红外光谱,多元掺假,模型优化,
英文关键词:camellia oil,near infrared spectroscopy,adulteration detection,multiple adulteration,model optimization,
发表日期：2019-10-21
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